臺灣博碩士論文加值系統

This thesis comprises four parts. The first part describes the synthesis of fan shape Alkoxy benzyl and aryl functionalized imidazolium salt. The liquid crystal behavior and self-assembly property were discussed.

In the second part, the liquid crystalline gold nanoparticles were prepared. To synthesize AuNPs via modified the Schiffrin’s two-phase method with imidazolium salt without additional stabilizing agent is reported. These AuNPs show good thermal ability and liquid crystalline SmA behavior. The temperature dependent SPR bands are observed for these AuNPs.

In continuation to our previous works are present in the third parts. This work collaborates with Josh Y. Z. Chiou, parts of data have been presented in the doctoral thesis. In this chapter, Ag(I)- and Au(I)-NHC complexes were synthesized. Thermal and photoluminescence properties of these complexes were studied. The gold compound shows different emission colors as crystal, soft materials, and thin film. Results of PXRD, Raman and IR studies suggest that a stronger Au-Au interaction has a smaller emission energy, and comes with weaker hydrogen bonding and hydrophobic interactions.

Abstract 1
Chapter 1. General Introduction 3
1.1 Introduction to Liquid Crystals 3
1.2 Introduction to nanoparticles 9
1.3 Introduction to N-heterocyclic carbene 11
Chapter2. Fan Shape Ionic Liquid Crystals of Alkoxy Benzyl Functionalized Imidazolium Salts 13
2.1 Abstract 13
2.2 Introduction 14
2.3 Synthesis 16
2.4 Results and discussion 19
2.4-1 Thermal behavior 19
2.4-2 Powder X-ray study 26
2.5 Conclusion 32
2.6 Experimental section 33
Chapter3. Gold Nanoparticle Liquid Crystal Composites: Preparation, Characterization and Surface Plasmon Resonance Coupling Behavior. 41
3.1 Abstract 41
3.2 Introduction 42
3.3 Method 44
3.3-1 Synthesis of imidazolium tetrachloroaurate salt 44
3.3-2 Preparation of gold nanocomposites 44
3.4 Results and discussion 46
3.4-1 Characterization of gold nanocomposites 46
3.4-2 Thermal behaviors of gold nanocomposites 48
3.5 Conclusions 62
3.6 Experimental section 63
Chapter 4. Photoluminescence of Self-assembled Ag(I) and Au(I) N-heterocyclic Carbene Complexes. Interplay the aurophilic, hydrogen bonding and hydrophobic interactions. 67
4.1 Abstract 67
4.2 Introduction 68
4.3 Synthesis 70
4.4 Results and discussion 72
4.4-1 Crystal structure 72
4.4-2 Thermal behavior 75
4.4-3 Photoluminescence behavior 82
4.5 Conclusions 91
4.6 Experimental section 92
Chapter 5. References 113

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