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Structural ceramic (also named Engineering ceramic) is a newly developedmaterial. Compared with metal for structure, it demonstrates manyexcellent physical and mechanical properties. Such as low density, lowcoefficient of expansion,low heat transfer coefficient, high Young'smodulus, high hardness, high compress strength, and good corrosion, oxidization,and creep resistance. Howrver, extreme brittleness is the primany obstacleto its application in engineering. Alumina is the typical material of ceramic. It is execellent for its high srengthand good ability to resist corrosion and oxidization. However,alumina alsopossess the weakness of low toughness.By adding reinforcement, its strengthand toughness can be improved. For example, the fracturetoughness can be increased by adding the metallic reinforcement. However, theoxidization resistance and the property of low density will be sacrificed.Therefore, it will be a target for researchers to choose areinforcement that will improve the weaknesses of the material and keep itselementary properties at the same time. Owing to its low density,easy to conduct heat, and excellent oxidization resistance,NiAl is chosen as a reinforcement in this study. To make a sample, we add NiAl particleinto alumina matrix evenly, from the mixed powder into the initial sample bydie-pressing method, and then sinter it in argon atmosphere at 1500℃. After sintering and milling, we proceed the following experiments: phase identificatinoby X-ray, measurement of mechanical and physical properties (including density,flexural strength, and fracture toughness)in room temperature, strength and toughnessof the samples after oxidization, and properties of the composite after thermalshock. By observing the microstructure of the samples, We tempt to find out thecauses that effect strength and toughness of the composit. Because of the complexity of making ceramic materials and time consumingprocess, we try to use the remaining material with other materials glued toboth ends to reduced the processing time and procedure.Thus, we can reusethe material and conduct the experiments repeatedly. Meanwhile, we comparethe data with that we got from experiment by standard sample. key words:fracture toughness, NiAl metallic compound ,methanical properties,
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