臺灣博碩士論文加值系統

本研究以鋁薄片作為基材，經由陽極氧化法製備具有週期性規則排列之蜂巢狀多孔結構氧化鋁模板。製備模板的電解液分硫酸及草酸兩種，利用草酸所製備的氧化鋁模板平均孔徑大小為50~70 nm，而硫酸約為20~40 nm。我們利用這兩種模板來填充單一金屬奈米線，填充的方式是使用電化學沈積法，經由電子顯微鏡觀察奈米線填充結果，並使用X 光能量散譜儀做奈米線之元素定性與定量分析，另使用X 光單晶繞射儀來鑑定樣品中的結構。

In this work, we use aluminum foil to be substrate to fabricate periodic nanopore arrangement in porous alumina template using an anodization. We use two kinds of electrolytes to fabricate templates. The two kinds of
electrolytes are oxalic acid and sulfuric acid. The average pore diameter of oxalic AAO is 50~70 nm, and the pore diameter of sulfuric AAO is about 20~40 nm. We use two kinds of templates to fill the one elemental metal nanowire by electrodeposition. We use X-ray and EDS to investigate two characterization and quantitative analysis of the metal nanowire arrays.

致謝
中文摘要
英文摘要
目錄
圖目錄
第1章 序論
1.1 前言
1.2 研究動機與目的
第2章 文獻回顧
2.1 多孔性結構之氧化鋁模板
2.1.1 氧化鋁奈米多孔模板的結構特徵
2.1.2 氧化鋁奈米多孔模板的成長機制
2.1.3 氧化鋁奈米多孔模板的製備變因
2.1.4 氧化鋁奈米多孔模板製備一維奈米結構材料
2.2 金屬奈米線的合成
參考文獻

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