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研究生:郭哲瑋
研究生(外文):Che-Wei Kuo
論文名稱:同步震動銲接之特性與機構研究
論文名稱(外文):Characteristics and Mechanisms of Simultaneous Vibration Welding
指導教授:吳威德吳威德引用關係
學位類別:博士
校院名稱:國立中興大學
系所名稱:材料科學與工程學系
學門:工程學門
學類:綜合工程學類
論文種類:學術論文
論文出版年:2008
畢業學年度:96
語文別:中文
論文頁數:84
中文關鍵詞:AISI 304Inconel 690振動應力消除振動銲接殘留應力
外文關鍵詞:AISI 304Inconel 690Vibratory stress reliefVibration weldingResidual stress
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本論文研究振動銲接特性與其機構,實驗採用AISI 304與Inconel 690兩種材料進行振動銲接。
因AISI 304在冷卻過程中會發生固態相變化,因此AISI 304用來研究振動銲接的特性。使用氬銲製程。實驗發現振動銲接造成細緻的δ-ferrite結構、均勻的成分分佈、較低的殘留應力與δ-ferrite含量。振動銲接的成核數量比無振盪高出許多,約3.5倍,會使δ-ferrite晶粒細化。此外因為δ→γ屬於擴散型相變化,δ-ferrite細化後擁有較大的表面積,結果在同樣的冷卻條件下可以減少一半的殘留δ-ferrite含量。成分的差異由EDS分析與彩色腐蝕的顏色分佈可以發現,振動銲接的試片擁有相對均勻的成分分佈。殘留應力方面,無振盪為262MPa,同步振盪銲接殘留應力降低到206MPa。
再經由比對銲接後進行應力消除的試片,其共同的特徵是X-ray繞射峰半高寬增大,排除應力與晶粒大小的影響後可以確認是疊差密度提高。整合文獻的發現推測,振動應力消除是因為完整差排分解為部分差排而降低殘留應力,這個機構可以解釋絕大部分振動應力消除發生的現象。
Inconel 690由於其凝固過程直接從液態凝固成為γ沃斯田鐵相,就不再發生相變化,可以保留振動凝固的組織,適合用來研究振動銲接的凝固機構。使用點銲與擺弧銲接來研究振動銲接的凝固機構,實驗發現沿著[001]振盪會導致液態原子析出在樹狀晶(dendrite)的(001)上,並沿著[001]快速成長,而當沿著[010]則導致大量的核析出在樹狀晶(010)上,形成大量且密集的第二枝臂(secondary dendrite arm),而這樣大量成核的結果導致細小的組織。另一方面擺弧銲接的結果顯示,無振盪的銲道晶粒因為磊晶成長在熔融線的前後晶粒的方向是連續成長的,而振動銲接在熔融線的前後晶粒的方向卻僅有平行振動方向能夠穿越熔融線,這個結果說明,振動銲接會造成銲道晶粒選擇性的成長,允許晶粒在振動同方向上的成長,而抑制垂直振動方向的成長,但振動銲接熔融線前後水平成長的晶粒並無延續方向成長,而在熔融線之後形成新的成長方向,所以在X-ray繞射的圖形上有3個明顯的繞射峰,而無振盪卻僅有一個。
這整個研究說明振動銲接不一定造成結構紊亂,事實上振動銲接會造成凝固組織有選擇方向性的凝固,當晶粒已經開始成長凝固時,振動並不能夠改變晶粒成長方向,而是在熔融後再凝固時才能形成新的方向。
This study investigates the characteristic and mechanisms of vibration welding. Two material AISI 304 and Inconel 690 were used for vibration welding.
AISI 304 represents the material which phase transformation occurs during solidifying to room temperature. AISI 304 was welded by GTAW to investigate the characteristics. The vibration weld shows a very small δ-ferrite structure, uniform composition distribution, less residual stress (from 262 to 206 MPa) and less δ-ferrite content relative to the weld without vibration. These results illustrate that the vibration increased the quantity of nucleation for about times 3.5 and the amount of δ-ferrite caused a grain refined structure. The fine structure offers a great surface for the diffusion phase transformation of δ→γ which reduce half content of δ-ferrite. Compare the samples of vibration welding and vibrate after welding, vibration-induced stacking faults are identified as the major cause of the line broadening of X-ray diffraction profile. Correlating the literature and the result in the study, the mechanism of vibratory stress relief can be represented as the breakdown of dislocation into a pair of partial dislocations. This mechanism can comprehensively explain all the phenomena that take place during vibratory stress relief.
To evaluate the crystal growth characteristics of vibration welding, Inconel 690 were welded when subjected to spot and arc oscillation with vibrations. Its primary γ-phase solidifies from the liquid state and cools to room temperature without any other phase transformation. Therefore, the solidifying structure will be completely retained for follow-up investigation. Results shows, if vibrated vertically, the vibration direction follow [001], and finally, the atoms will fit into the (001) plane and growth quickly. However, when the vibrations are along [001], the (010) planes receive liquid atoms and grow and they appear as highly concentrated secondary dendrite arms. Base on the highly concentrated secondary dendrite arms, it performs a grain refinement structure. On the other hand, the results of arc oscillation vibration illustrate that vibration in selected direction transmits to weld pool and excitates it in the same direction. The observation of the microstructure of the welds indicates that if the grain growth direction is parallel to the vibration direction, the grain can continue epitaxial grow and maintain its orientation. On the contrary, if the grain growth orientation is perpendicular to the vibration direction, the growth will be restrained, and the grain will cease its growth at the edge of the fusion line. Hence, new grains and orientations are formed after the second pass welding. This is the reason why vibration welding has the more preferred orientation over vibrationless welding.
The study interprets that vibration welding not always create a chaos structure certainly, actually, it selected direction transmits to solidify the grain structure. While grain growth starts, vibration can not change grain growth direction but start forming new growth directions from fusion line.
摘要 I
Abstract III
總目錄 VI
圖目錄 VIII
表目錄 X
第一章 前言 1
第二章 文獻回顧 3
2-1 振盪理論 3
2-1.1 振動消除應力理論 3
2-1.2 振動應力消除機構 6
2-2 振動銲接 9
2-3 AISI 304沃斯田鐵系不�袗�銲接 16
2-4 鎳基690合金 20
2-5 影響X-ray繞射峰形狀的因素 21
2-6 X-ray繞射測量應力 23
三 實驗步驟 25
3-1 AISI 304振動銲接 28
3-1.1 δ-ferrite觀察、成分與含量測量 30
3-1.2 殘留應力測量 31
3-1.3 AISI 304 晶體結構分析 32
3-2 Inconel 690垂直/水平振動銲接 33
3-2.1 Inconel 690垂直/水平振動銲接 34
3-2.2 Inconel 690振動擺弧銲接 35
3-2.3 波形對振動銲接的晶體結構影響 36
3-2.4 Inconel 690 晶體結構分析 37
第四章 結果與討論 39
4-1 AISI 304不�袗�銲道結構 39
4-2 振動銲接對AISI 304不�袗�銲道的成分分佈影響 42
4-3 δ-ferrite含量變化 44
4-4 殘留應力與應力消除機構探討 46
4-5 振動對晶體結構影響 53
4-5.1點銲—垂直/水平振動方向對晶體成長的影響 54
4-5.2 Inconel 690擺弧銲接-不同振動方向對晶體成長的影響 64
4-6 振幅波形的影響 69
第五章 結論 73
第六章 參考文獻 75
著作 83
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