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研究生:呂宛玲
研究生(外文):Wan-Ling Lu
論文名稱:以氣相層析嗅聞法(GC-Sniffing)及電子鼻(E-nose)檢測蜆精氣味之比較
論文名稱(外文):Comparison on Aroma Profile of Clam Essence Measured with GC-Sniffing and Electronic Nose
指導教授:孫寶年孫寶年引用關係
指導教授(外文):Bonnie Sun Pan
學位類別:碩士
校院名稱:國立臺灣海洋大學
系所名稱:食品科學系
學門:農業科學學門
學類:食品科學類
論文種類:學術論文
論文出版年:2009
畢業學年度:97
語文別:中文
論文頁數:74
中文關鍵詞:氣相層析嗅聞法電子鼻蜆精氣味
外文關鍵詞:GC-SniffingE-noseclam essenceodor
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摘 要
台灣蜆 (Freshwater clam, Corbiclular fluminea) 為台灣地區主要淡水養殖貝類,民間普遍以熬蜆湯以滋補身體,並認為有保肝效果。目前市面上已有蜆精產品,但氣味不良,故本實驗以 GC/MS分析蜆精之氣味化合物, E-nose建立蜆精氣味之指紋圖,以便快速進行蜆精氣味之品質管理及控制腥氣。
由 E-nose建立各樣品之氣味指紋。樣品 (E) 中含有氣味強之添加物,其氣味指紋強度大於其他樣品,剔除樣品 (E) 後轉換成 PCA 分析得知樣品氣味主成分差異性為 99.67%;以 SQC 分析,樣品 (D)、(F) 距離以樣品 (A)為氣味品質標準區之範圍最遠,其氣味品質與品質標的樣品差異最大,進一步可應用於生產線上,對於不同批次之產品進行管控,以確保產品之品質。雷達圖當中感應器 PA2、T30/1 及 T70/2 在各樣品中差異明顯,利用感應器敏感氣體表推測結果與GC/MS 相符合,而P10/1、P10/2 及 P40/1 感應器對於吸附樣品氣味並無太大差異。
樣品進行 GC 分析及嗅聞,市售樣品 (A) - (D) 和 (F) 進行嗅聞,可聞到烤味 (R.I. = 1204) 、甜味、清涼味 (R.I. = 1501) 、花香味 (R.I. = 1627) 、燒烤味、胡椒味 (R.I. = 1641) ;市售樣品 (E) 可聞到刺激、硫味 (R.I. = 977、1517) 。生蜆肉 (G) 的脂肪酸中 PUFA占總脂肪酸 17.89 %,當中以 C18:3 n-3 含量最高,C22:6 n-3含量次之,可作為 LOX 氧化反應產生氣味。自製蜆精 (H) 因加溫造成 LOX 失去活性,無法與脂質作用,且揮發性高之氣味化合物已揮發,導致氣味化合物含量低。以GC/MS 鑑定揮發性成份,樣品中醇類比例最高。將市售樣品與生蜆肉 (G) 及自製蜆精 (H) 比對,發現樣品 (G) 及(H) 並未測出碳氫化合物及含氮、含硫化合物,在此認定為添加之香氣配料。市售樣品與生蜆肉 (G) 和自製蜆精 (H) 比對,市售樣品含有 1-nonanol (7/8,油味、草味)、l-dodecanol (5/8,油味、蠟味) 及 benzaldehyde (4/8,杏仁味、燒烤味)。
Abstract
Freshwater clam (Corbiclular flminea) is the major freshwater cultivated bivalvia in Taiwan. In addition, local people believe that the soup made with freshwater clam has hepatoprotective activity. There are many clam essences in market, but the odor of those products is hard to accept by consumer. The purpose of this study was using GC/MS to analysis the odor of clam essences, establishing fingerprint of sample and quickly controlling the odor quality of clam essence by E-nose
E-nose plot showed that sample (E) was stronger than the other 5 commercial clam essences products in 6 volatile attributes. Its principal component analysis (PCA) differed at 99.67% level from the other products, which showed similar profile that was hard to distinguish from each other. Statistical quality control (SQC) of clam essence odor was assessed product odor quality control, can apply on the production line. Sample (D) and (F) were separate from sample (A) as normal area in SQC plot. Comparing with sensitive gas of sensor, PA2, T30/1 and T70/2 sensors in radar plot of clam essences showed alcohols having significantly different and P10/1, P10/2 and P40/1 sensors didn’t.
Analysis samples with GC/FID and GC-sniffing,that we can smell burnt (R.I. = 1204), sweet, mint (R.I. = 1501), flower (R.I. = 1627), burnt pepper (R.I. = 1641) in sample (A), (D) and (F); sulfurous (R.I. = 977、1517) in sample (E). There were 17.89 % PUFA in flash clam meat (G), could product odor through LOX oxidation. The odor concentration of lab-made clam essence was low, because temperature cause LOX deactivate and make high volatile compounds evaporated
Proportion of volatile alcohols was highest in samples identifying by GC/MS. Some hydrocarbons, nitrogen and sulfur compounds were established as additive because haven’t been detected in clam meat (G) and Lab-made clam essence (H), There were 1-nonanol (fatty, green)、l-dodecanol (fatty, waxy) and benzaldehyde (almond, burnt sugar) in commercial clam essence.
目錄
中文摘要 i
英文摘要 iii
圖目錄 v
表目錄圖 vi
壹、 前言 1
貳、 文獻回顧 3
一、 食品風味 3
1. 食品風味之形成 3
2.1 醇類 (alcohols) 3
2.2 醛類 (aldehydes) 4
2.3 酮類 (ketones) 5
2.4 酸類 (acids) 6
2.5 酯類 (esters) 6
2.6 雜環化合物 6
(1) 環氧化合物 7
(2) 含氮化合物 7
(3) 含硫化合物 8
二、 水產品風味 9
1. 魚 9
2. 蝦類 10
3. 貝類 11
三、 氣味分析方法 12
1. 氣相層析嗅聞裝置 13
2. 電子鼻 14
參、 材料與方法 17
一、 材料 17
1. 生蜆肉 17
2. 自製蜆精 17
3. 市售蜆精 17
4. SPME吸附纖維 17
二、 氣味成份分析 19
1. 氣味成份萃取 19
1.1. 固相微量萃取法 (solid-phase microextraction, SPME) 19
1.2. MonoTrap 法 20
2. 氣相層析 (Gas chromatography, GC) 20
3. 氣相層析嗅聞法 (GC-Sniffing) 20
4. 滯留指數 (Retention index, R.I.) 之測定 21
5. 氣液相層析-質譜儀 (GC/MS) 分析 21
三、 電子鼻氣味分析 22
1. 氣味成份萃取 22
2. 電子鼻 (electronic nose, E-nose) 22
四、 脂肪酸分析 25
1. 脂質萃取 25
2. 氣相層析分析 25
肆、 結果與討論 27
一、 蜆精氣味品質管控 27
1. 電子鼻雷達圖 27
2. 氣味指標成份 34
二、 蜆精氣味化合物組成 36
1. 氣味化合物SPME 吸附纖維之選擇 36
2. 氣味化合物之分離 39
2.1. 生蜆肉 39
2.2. 自製蜆精 39
2.3. 市售蜆精 45
3. 氣味化合物之鑑定 53
2.1. 碳氫化合物 53
2.2. 醇類 53
2.3. 醛類 54
2.4. 酮類 55
2.5. 含氮及含硫化合物 55
伍、 結論 60
陸、 參考文獻 62
陸、 參考文獻
Association of Official Agricultural Chemists (1995) Offical Methods of Analysis, 16th Eds., Association of Official Analytical Chemistry Washington, DC, U.S.A.
Amano A., (1985) Sulfur containing aroma compounds in natural products. Koryo, 146:37-46.
Alasalvar C., T. Aishima and P.C. Quantick (1995) Dynamic headspace analysis of volatile aroma compounds of fresh and deteriorated mackerel (Scomber scombrus). Food Sci. Technol. Int. 1:125–127.
Alasalvar C., K. D. Taylor, and F. Shahidi (2005). Comparison of volatiles of cultured and wild sea bream (Sparus aurata) during storage in ice by dynamic headspace analysis/gas chromatography–mass spectrometry. J. Agric. Food Chem., 53: 2616–2622.
Artacho Martin-Lagos R., M. F. Olea Serrano, and M. D. Ruiz Lopez (1995) Determination of organic sulfur compounds in garlic extracts by gas chromatography and mass spectrometry. Food Chem., 53:91-93.
Bachinger T., D. Rises, R.K. Eriksson, and C-F. Mandenius (2000) Monitoring cellular state transitions in a production–scale CHO-cell processs using an electronic nose. J.Biothchnol., 76:61-71.
Bachinger T., C-F. Mandenius, G. Striedner, F. Clementschitsch, E. Durschmis, M. Cserian-Puschmann, O. Doblhoff-Dier and K. Bayer (2001) Noninvasive detection of the metabolic burden on recombinant microorganisms during fermentation processes. J. Chem. Technol. Biotechnol., 6:885-889.
Bachinger T., U. Riese, R.K. Erilsson and C-F Mandeius (2002) Gas senser arrays for early detection of infection in mammalian cell culture. Biosens. Bioelectron., 17:395-403.
Bachinger T., P. Martensson, and C-F Mandenius (1998) On-line estimation of biomass and specific growth rate in a recombineant Escherichia coli batch cultivation using a chemical multisensory array. J. Biothchnol., 60:55-66.
Bailey M.E. (1983) The Maillard reaction and meat flavor. Ch.5. in G.R. Waller and M.S. Feather, editors. The Maillard reaction in Foods and Nutrition, American Chemical Society, Washington, DC, USA, pp.169-183.
Berna A.Z., J. Lammertyn, S. Saevels, C. Di Natale and B.M. Nicolai, (2004) Electronic nose systems to study shelf life and cultivar effect on tomato aroma profile. Sensor Actuat. B-Chem., 97:324-333.
Bicchi C., C. Cordero, L. Liberto, P. Rubiolo and B. Sgorbini (2004) Automated headspace solid-phase dynamic extraction to analyse the volatile fraction of food matrices. J. Chromatogr. A., 1024:217-226.
Calkins C.R., and J.M. Hodgen, (2007) A fresh look at meat flavor. Meat Sci., 77:63-80.
Carpino F., V. M. Moretti, F. Bellagamba, G. M. Turchini, M.L. Busetto, I. Giani, M.A. Paleari and M. Pazzaglia (2008) Fatty acid composition and volatile compounds of caviar from farmed white sturgeon (Acipenser transmontanus). Anal. Chim. Acta., 617:139-147.
Chaintreau A. (2001) Simultaneous distillation-extraction: from birth to maturety-review. Flavour Frag. J., 16:136-148.
Chen C.F. and C.S. Lin (2003) Hepatoprotective effects of clam extract supplementation on subacute hepatitis induces by carbon tetrarchloride in rate. Taiwanese J. Agric. Chem. Food Sci., 41:159-166.
Chen T. Y., B. C. Lin, M. S Shiao and B. S. Pan (2008) Lipid-lowering and LDL-oxidation inhibitory effects of aqueous extract of fresh-water clam (Corbicula fluminea)-using tilapia as an animal model. J. Food Sci. 73:148-154.
Chiba A. (1990) development of the TGS gas sensor. Chem. Sens. Technol., 2:1-18.
Curioni P. M. G. and J. O. Bosset (2002) Key odorants in various cheese types as determined by gas chromatography-olfactometry. Int. Dairy J., 12:959-984.
Dewettinck T, K. Van Hege and W. Verstraete (2001) The electronic nose as a rapid sensor for volatile compounds in treated domestic wastewater. Wat. Res., 35:2475-2483
Drawert F. and N. Christoph (1984) Significance of the sniffing-technique for the determination of odour thresholds and detection of aroma impacts of trace volatiles. In Schreier.P. editors, Analysis of Volatiles Walter de Gruyter, New York, pp. 269-292
Durnford E. and F. Shahidi (1998) Flavour of fish meat. In F. Shahidi editor. Flavour of mea, meat products and seafoods, London:Blackie A&P. pp.131-158
Fuller G.H., R. Steltenkamp and G.A. Tisserand (1964) The gas chromatograph with human sensor. Ann. NY. Acad. Sci., 116:711–724.
Ganeko N., M. Shoda, I. Hirohara, A. Bhadra, T. Ishida, H. Matsuda, H. Takamura, and T. Matoba (2008) Analysis of volatile flavor compounds of sardine (Sardinops melanosrica) by solid phase microextraction. J. Food Sci., 73:83-88.
Gardner J. W. and P. N. Bartlett (1994) A brief history of electronic nose. Sens. Actuators B. 19:211-220.
Gardner J. W. and P. N. Bartlett (2000) Electronic noses: principles and applications, Meas. Sci. Technol., 11:1087-1087.
Gostelow P., S. A. Parsons and R. M. Stuetz (2001) Odour measurements for sewage treatment works. Wat. Res. 35: 579-597.
Grimm C.C., S.W. Lloyd, R. Batista and P.V. Zimba, (2000) Using microwave distillation-solid-phase microextraction-gas chromatography–mass spectrometry for analyzing fish tissue. J. Chromatogr. Sci., 38:289–296.
Gu L.L., R.J. Yang and Q. Chen (2004) Determination of flavor substances in oyster by SPME coupled to gas chromatography,. China Condiment , 10: 43–46.
Guadarrma A., J.A. Fernandez, M. Iniguez, J. Souto and J.A. Saja (2000) Array of conducting polymer sensors for the characterization of wines. Ana. Chim. Acta., 411:193-200.
Hatanaka A., T. Kajiwara and T. Harada (1975) Biosynthetic pathway of cucumber alcohol: trans-2,cis-6-nonadienol via cis-6-nonadienal. Phytochemistry, 14:2589-2592.
He C.S. and H. Kato (1985) Flavor of fermented product of Antartic Krill prepared by modified method (odor of fermented small shrimp part Ⅵ). Nippon Shokuhin Kogyo Gakkaishi, 32:274-280.
Hebard C.E., G.J. Flick and R.E. Martin (1982) Occurrence and significance of trimethylamine oxide and its derivatives in fish and shellfish. In: Marin, R.E., Flick G.J., Hebard C.E. and Ward D.R. editors. Chemistry and Biochemistry of Marine Food Products, AVI Publishing CO., Westport CT, pp.149-305.
Hibbert D.B. (1999) Electronic noss for sensing and analyzing industrial chemicals. In G.A. Bell and A.J. Watson editors, Taste and Aromas:the Chemical Senses in Science and Industry. UNSW Press: Sydney, Astralia, pp.180-188.
Hirano T., C.H. Zhang, A. Morishita, T. Suzki and T. Shirai (1992) Identification of volatile compounds in ayu fish and its feeds. Nippon Suiuan Gakk., 58:547-557.
Hsieh T. C. Y., U. Tanchotikul, and J. E. Matiella (1988) Identification of Geosmin as the major muddy off-flavor of Louisiana brackish water clam (Rangia cuneata). J. Food Sci., 53:1228-1229.
Hsieh R. J., amd J. E. Kinsella, (1989). Lipoxygenase generates specific volatile carbonyl compounds in fish tissues. J. Agric. Food Chem., 37:279–286.
Hu SP, B.S. Pan, (2000) Modification og fish oil aroma using a macroalgal lipoxygenase. J. Am. Oil Chem. Soc. 77:343-348.
Huang Y.Y., H. Huang, T.C. Hour, B.S. Pan, Y.C. Liu and M.H. Pan (2006) Apoptosis-inducing active components from Corbicula Fluminea through activation of caspase-2 and production of reactive oxygen species in human leulemia HL-60 cells. Food Chem. Toxicol., 44:126-1272.
Iglesias J., and I. Medina (2008) Solid-phase microextraction method for the determination of volatile compounds associated to oxidation of fish muscle. J. Chromatogr. A 1192:9-16.
Institute of food technologists, (1975) Shelf-life of Foods. Food Aust., 27:315-19.
Jacobsen C., M. Timm and A. Meyer, (2001) Oxidation in fish oil enriched mayonnaise: ascorbic acid and low ph increase oxidative deterioration. J. Agric. Food Chem. 49:3947-3956
Jo?nsdo?ttir R., M. Bragado?ttir and G.O. Arnarson, (2005) Oxidatively derived volatile compounds in microencapsulated fish oil monitored by solid-phase microextraction (SPME) J. Food Sci. 70:C433-440.
Josephson D.B., R.C. Lindsay and D.A. Stuiber (1984a) Biogenesis of lipid-derived volatile aroma compounds in the emerald shiner (Nortropis atherinoises). J. Agric. Food Chem., 32:1347-1352.
Josephson D.B., R.C. Lindsay and D.A. Stuiber (1984b) Identification of compounds characterizing the aroma of fresh whitefish. J. Agric. Food Chem., 31:326-330.
Josephson D.B., R.C. Lindsay and D.A. Stuiber (1985) Volatile compounds characterizing the aroma of fresh atlantic and pacific oysters. J. Food Sci., 31:326-330.
Kawai T. (1996). Fish flavor. Crit. Rev. Food Sci., 36:257–298.
Kim H.S., B.H. Kim and Y.D. Cho (1998) Purification and characterization of monomeric lysine decarboxylase from soybean (Glycine max) Axes. Arch. Biochem. Biophy., 354:40-46.
Kobayashi, A., K. Kubota, M. Iwamoto and H. Tamura (1989) Syntheses and sensory characterization of 5,8,11-tetradecatri-en-2-one isomers. J. Agric. Food Chem., 37:151-154.
Kong Z.I., L.C. Chiang, F. Fang, K. Shinohara and P. Pan (1997) Immune bioactiveity in shelfish toward serum-free cultured human cell lines. Biosci. Biotech. Bioch., 61:24-28.
Kreij K., C-F Mansenius, J.J. Clemente, A.E. Cunha, S.M.S. Montero and M.J.T. Carrondo (2005) On-line detection of microbial contaminations in animal cell reactor cultures using an electronic nose device. Cytotech., 48:41-58.
Kuo J.M. and B.S. Pan (1992) Occurrence of properties of 12-lipoxygenase in the hemolymph (Penaeus japonicas Bate). J. Chinese Biol. Soc., 21:9-16.
Kuo J.M., A. Hwang, H.H. Hsu and B.S. Pan (1996) Preliminary identification of lipoxygenase in algae (Enteromorpha intestinalis) for aroma formation. J. Agric. Food Chem., 44:2073-2077.
Leon, A., A. Chica, J. Garcia-Raurich, and F. Centrich (1994) Determination of trimethylamine in fish by flow injection analysis. Quim. Anal. 13:78-81.
Lindsay R.C. (1990) Fish flavors. Food Rev. Intl., 6:437-455.
Lindsay R.C. (1996) Flavor, In O.R. Fennema editor, Food Chemistry 3rd. Marcel dekker, Inc. NY, U.S.A. pp. 723-762.
Liu S.-Q., R. Holland and V.L. Crow, (2004) Esters and their biosynthesis in fermented dairy products: a review. Int. Dairy J., 14:923–945.
Ma N.T., C.C. Chyau and B.S. Pan, (2004) Fatty acid profile and aroma compounds of the lipoxygenase –modified chicken oil. J. Am. Oil Chem. Soc., 81:921-926.
Maga J.A., (1976) Lactones in foods. Crit. Rec. Food Sci., 14:1-56.
Macleod G. (1998) The flavor of beef, In F. Shahidi editor, Flavour of mea, meat products and seafoods. London:Blackie A&P, pp.27-60.
Mandenius C-F., T. Eklov and I. Lundstrom, (1996) Sensor fusion with on-line gas emission multisensory arrays and standard process measuring devices in baker’s yeast manufacturing process. Biotechnol. Bioeng., 55(2):427-438.
Mandenius C-F., A. Hagman, F. Dunas, H. Sundgren and I. Lndstrom, (1998) A multisensory array for visualizing continuous state transition in biopharmaceutical processes using principal component analysis. Biosens. Bioelectron., 13(2):193-199.
Morales M.T., J.J. Rios, and R. Aparicio (1997) Changes in the volatile composition of olive oil during oxidation:flavors and off-flavors. J. Agric. Food Chem., 45:2666-2673.
Morgan M.E., (1970) Microbial flavor defects in dairy products and methods for their simulation. II. Fruity flavour, J. Dairy Sci., 53: 273-275.
Mottram D.S., (1998) Flavour formation in meat and meat products: A review, Food Chem. 62:415-424.
Mottram D.S. and H.R. Mottram, (2002) An overview of the contribution of sulfur-containing compounds to the aroma in heated foods. In: G.A. Reineccius and T.A. Reineccius, Ed., Heteroatomic aroma compounds, ACS Symposium, Washington, DC, pp. 73-92.
Nawar W.W. (1985) Thermal and radiolytic decomposition of lipids. Ch.3. in Chemical Changes in Food during Processing, T. Richardson and J.W. Finely, editors. Chapman & Hall, New York, USA, pp. 79-105.
Pan B.S. and J.M. Kuo (1994) Flavor of shellfish and kamaboko flavorants. In Shahidi, F. and Botta J.R. editors Seafoods: Chemistry, Processing Technology and Quality, Chapman & Hall, Great Britain, pp.85-114.
Pan B.S., J.R. Tsai, L.M. Chen and C.M. Wu (1997) Lipoxygenase and sulfur-containing amino acids in seafood flavor formation. in Flavor and Lipid Chemistry of Seafoods., ed F. Shahidi and K.R. Cadwallader. Amer. Chem. Soc. Symp. Series., 647:64-75.
Papadopoulos C.A., D. Vlachos, and J.N. Avaritsiotis (1996) Comparative study of various metal-oxide-based gas-sensor architectures. Sensor Actuat. B-Chem., 32:61–69.
Pennarun A. L., C. Prost and M. Demaimay (2002) Identification and origin of the character-impact compounds of raw oyster Crassostrea gigas. J. Sci. Food Agric., 82:1652-1660.
Persaud K. and G.H. Dodd, (1982) Analysis of discrimination mechanisms in the mammalian olfactory system using a model nose. Nature, 299:352–355.
Piveteau F., S. L. Guen, G. Gandemer, J. P. Baud, C. Prost, and M. Demaimay (2000) Aroma of Fresh Oysters Crassostrea gigas: Composition and Aroma Note. J. Agric. Food Chem., 48:4851-4857.
Prost C., A. Hallier, M. Cardinal, T. Serot and P. Courcoux, (2004) Effect of storage time on raw sardine (Sardina pilchardus) flavor and aroma quality, J. Food Sci., 69:198–203.
Ragazzo-Sanchez J.A., P.Chalier, D. Chevalier, M.Calderon and C. Ghommidh (2008) Identification of differential alcohol beverages by electronic nose coupled to GC. Sensor Actuat. B-Chem., 134:43-48.
Robert C. L. (1996) Flavor. CH. 11. In Food Chemistry, R.F. Owen editor, Marcel Dekker, Inc., N.Y., U.S.A. pp.723-765
Ross C. F. and D. M. Smith (2006) Use of volatiles as indicators of lipid oxidation in muscle foods. Compr. Rev. Food Sci. Food Safe., 5:18–25.
Saevel S., C. Di Natale., A.Z. Berna , E. Veraverbeke, J. Lammertyn, and B.M. Nicolai (2003) Electronic nose as a non-destructive tool to evaluate the optimal harvest sate of apples. Postharvest Biol. Technol., 30:3-14.
Saevel S., J. Lammertyn, A.Z. Berna , E. Veraverbeke, C. Di Natale., and B.M. Nicolai (2004) An electronic nise and a mass sprctrometric based electronic nose for assessing apple quality during shelf life. Postharvest Boil. Technol., 31:9-19.
Sakakibara H., T. Yanai, I. Yajima and K. Hayashi (1988) Changes in volatile flavor compounds of powdered dried bonito (Katsuobushi) during storage. Agr. Biol. Chem. Tokyo, 52:2731-2739.
Schaller E., J.O. Bosset and F. Escher (1998) ‘Electronic noses’ and their application to food. Lebensm. Wiss. Technol., 31:305-316.
Schomburg G., and G. Dielman (1973) Identification by means of retention parameters. J. Chromatogr. Sci., 11:151-158.
Shibamoto T., T. Akiyama, M. Sakaguchi, Y. Enomoto and H. Masuda (1979) A study of pyrazine formation. J. Agr. Food Chem., 27:1027-1031.
Spurvey S., B. S. Pan, and F. Shahidi (1998) Flavour of Shellfish. In F. Shahidi editor, Flavour of mea, meat products and seafoods London:Blackie A&P, pp.159-196
Tabor C.W., and H. Tabor (1984) Polyamines. Annu. Rev. Biochem., 53:749–90.
Tachihara T, S. Ishizaki, M. Ishikawa, and T. Kitahara (2004) Studies on the volatile compounds of roasted spotted shrimp. Chem. Biodivers. 1:2024-33.
Takeoka G. R., R. G. Buttery, L. C. Ling, R. Y. Wong, L. T. Dao, R. H. Edwards and J. J. Berrios (1998) Odor thresholds of various unsaturated branched esters. Lebensm. Wiss. Technol., 31:443–448
Tamura H.,H. Nakamoto, R.H. Yang and H. Sugisawa. (1995) Characteristic aroma compounds in green algae (Ulva pertusa) volatiles. Nippon Shokuhin Kagaku Kogaku Kaishi
Tanchotikul U., and T. C.–Y. Hsieh (1991) Analysis of volatile components in steam Rangia cuneata by dynamic headspace sampling and simultaneous distillation and extraction. J. Food Sci., 56(2):327-331.
Tanchotikul U. and T. C. Y. Hsieh (1989) Volatile flavor components in crayfish waste. J. Food. Sci., 54:1515-1520.
Taylor A.J. (2002) Food Flavor Technology. Sheffield Academic Press, UK, pp.210-251.
Toure A. and Z. Xiaoming, (2007) Gas chromatographic analysis of volatile compounds of guinean and Chinese ginger oils (Zingiber officinale) extracted by steam distillation. J. Agronomy, 6:350-355.
Tsai J.S., T.C. Lin, J.L. Chen and B.S. Pan (2006) The inhibitory effects of freshwater clam (Corbicula fluminea, Muller) muscle protein hydrolysates in angiotensin I converting enzyme. Process Biochem., 41:2276-2281.
Tsai J.C., Li W. F., and B.S. Pan (2008) Characterization and immobilization of marine algal 11-lipoxygenase from U;va fasciata. J. Am. Oil Chem. Soc., 85:731-737.
Varlet V, C. Prost and T. Serot (2007) Volatile aldehydes in smoked fish: Analysis methods, occurrence and mechanisms of formation. Food Chem., 105:1536–1556.
Vejaphan W., T.C.Y. Hsieh and S.S. Williams (1988) Volatile flavor components from boiled crayfish (Procambarus clarkii) tail meat. J. Food Sci., 53:1666-1670.
Vernin G., S. Chakib, S.M. Rogacheva, T.D. Obretenov and C. Parkanyi, (1998) Thermal decomposition of ascorbic acid. Carbohyd. Res., 1-15.
Varlet V., C. Prost, T. Serot, (2007) Volatile aldehydes in smoked fish: Analysis methods, occurence and mechanisms of formation. Food Chem., 105:1536-1556.
Wilkes J.G., E.D. Conte, Y. Kim, M. Holcomb and J.B. Suthertland (2000) Sample preparation for the analysis of flavors and off-flavors in foods. J. Chromatogr. A., 880:3-33.
Wu T.Z. (1999) A piezoelectric biosensor as an olfactory receptor for odour detection: electronic nose. Biosens. Bioelectron., 14:9-18.
Wu C.M., J.M. Kou and B.S. Pan (2002) Flavor Compounds In: Zdzis?aw E. Sikorski editors. Chemical and functional properties of food components 2nd , Boca Raton London, New York, Washington, D.C.
Wurzenberger M. and W. Grosh, (1984) The formation of 1-octen-3-ol from the 10-hydroperoxide isomer of linoleic acid by hydroperoxide lyase in mushrooms (Psalliota biospora). Biochimica et Biophysica Acta. 794: 25–30.
Yang Y.M., P.Y. Yang, X.R. Wang, (2000) Electronic nose based on SAW array and its odor identification capability. Sens. Actuators B 66:167–170.
Zhang Z., M.J. Yang and J. Pawliszyn (1994) Solid-phase microextraction. Anal. Chem., 66:844A-853.
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