研究中使用三種不同的方式合成銀鉛氧化合物，並製成電極以電化學方式進行反應，試圖改變其結構中的價態或者元素組成，藉此希望觀測到物理性質的改變。藉由電化學、XRD與ESCA分析後，推斷其可逆範圍的充放電是由於鉛氧層中的價態變化來平衡。

In this paper, three different routes have been adopted for the synthesis of silver lead oxide (Ag5Pb2O6). The synthesized material is then subjected to electrochemical reaction, anticipating the change in the valency of the constituent elements which result in changing the physical behavior with temperature. The prepared compound is made into a coin cell and the charge-discharge studies are carried out. ESCA analysis inferred the reversible charge-discharge range is due to the changes in the valency of lead oxide.

目錄 III
圖目錄 IV
表目錄 V
第一章 緒論 1
銀鉛氧化物簡介 1
第二章 實驗步驟 5
2.1 合成Ag5Pb2O6 5
2.2 組裝鈕扣型電池 6
2.3 藥品 7
2.4 儀器 8
第三章 結果與討論 13
3.1 銀鉛氧化物之合成結果 13
3.2 電化學實驗 22
第四章 結論 43
第五章 參考文獻 44

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