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研究生:江文賢
研究生(外文):CHIANG,WEN-HSIEN
論文名稱:直接成長二硫化鉬奈米片在咖啡渣製備的水合活性碳上並應用於電化學超級電容器
論文名稱(外文):Directly Growing MoS2 Nanoflakes on Hydrated Activated Carbon Prepared from Coffee Grounds and Applied in Electrochemical Supercapacitors
指導教授:高立衡高立衡引用關係
指導教授(外文):KAO,LI-HENG
口試委員:林鉉凱莊高樹高立衡
口試委員(外文):LIN,HSUAN-KAICHUANG,KAO-SHUKAO,LI-HENG
口試日期:2020-06-24
學位類別:碩士
校院名稱:國立高雄科技大學
系所名稱:化學工程與材料工程系
學門:工程學門
學類:化學工程學類
論文種類:學術論文
論文出版年:2020
畢業學年度:108
語文別:中文
論文頁數:79
中文關鍵詞:咖啡渣活性碳二硫化鉬電化學超級電容器
外文關鍵詞:Coffee groundsActivated carbonMolybdenum disulfideSupercapacitor
相關次數:
  • 被引用被引用:1
  • 點閱點閱:275
  • 評分評分:
  • 下載下載:0
  • 收藏至我的研究室書目清單書目收藏:0
摘要 I
Abstract III
誌謝 V
總目錄 VI
表目錄 X
圖目錄 XI
第一章 緒論 1
第二章 基本原理與文獻回顧 4
2-1 活性碳簡介 4
2-2 超級電容器(Super capacitor) 6
2-2-1 電雙層電容(EDLC) 7
2-2-2 偽電容(Pseudocapacitor) 8
2-3 二維層狀結構的材料應用於超級電容器之電極 9
2-4 TMDs複合材料合成 11
2-4-1 水/溶劑熱法 11
2-4-2 微波輔助和成法 11
2-4-3 噴塗法 12
2-5 MoS2特性 12
2-6 電化學原理與測量方法 13
第三章 實驗方法與步驟 17
3-1 實驗藥品 17
3-2 分析儀器及設備 18
3-3實驗流程 20
3-3-1 咖啡渣活性碳(Activated Carbon)之製備 20
3-3-2 活性碳二硫化鉬(AC/MoS_2)複合材料之製備 21
3-3-3 電極製備 22
3-4 材料分析儀器介紹 24
3-4-1 X光繞射儀(X-ray Diffractometer,XRD) 24
3-4-2 超高解析度熱場發射掃描式電子顯微鏡(Field Emission Scanning Electron Microscope,FE-SEM) 25
3-4-3 場發射穿透式電子顯微鏡(Field Emission Transmission Electron Microscope) 26
3-4-4 比表面積與孔隙度分析儀(Specific Surface Area and Poro Size Distribution Analyzer,BET) 26
3-4-5 恆電位/電流/交流阻抗儀(Potentiostat/Galvanostat/Fras) 31
3-5 電極之電化學性質 32
3-5-1 循環伏安曲線測量 32
3-5-2 計時電位曲線測量 33
3-6 電化學電容器之比電容計算 33
3-6-1 計時電位法 34
3-6-2 循環伏安法 34
3-7 電化學電容器之功率能量密度計算 35
3-8 交流阻抗分析 35
第四章 結果與討論 36
4-1 SEM&TEM材料表面結構 36
4-2 XRD材料晶像鑑定 49
4-3 Raman特徵峰鑑定 50
4-4 BET材料比表面積分析 51
4-5 電化學電性測試結果 53
第五章 結論 60
參考文獻 61


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