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研究生:林揆樺
研究生(外文):LIN, KUEI-HUA
論文名稱:藉由熱分析技術評估過氧化氫穩定劑之穩定功效
論文名稱(外文):Inhibiting Effect of Two Stabilizers on Decomposition of Hydrogen Peroxide via Thermal Analysis Method
指導教授:徐啟銘徐啟銘引用關係李樹華李樹華引用關係
指導教授(外文):SHU, CHI-MINLEE, SHUH-HWA
口試委員:王義文陳豐華游美利
口試委員(外文):WANG, YIH-WENCHEN, JIANN-RONGYOU, MEI-LI
口試日期:2020-07-16
學位類別:碩士
校院名稱:國立雲林科技大學
系所名稱:環境與安全衛生工程系
學門:工程學門
學類:環境工程學類
論文種類:學術論文
論文出版年:2020
畢業學年度:108
語文別:中文
論文頁數:80
中文關鍵詞:過氧化氫2010 水處理劑2-苯胺乙醇微差掃描熱卡計多頻道微量熱卡計
外文關鍵詞:Hydrogen peroxide1-Hydroxyethylidene-1,1-diphosphonic2-AnilinothanolDifferential scanning calorimetryThermal activity monitor III
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摘要 i
ABSTRACT ii
誌謝 iii
目錄 iv
表目錄 vi
圖目錄 vii
第一章 緒論 1
1.1 研究背景 1
1.2 研究目的 6
第二章 文獻回顧 7
2.1 過氧化氫應用 7
2.1.1 漂白 7
2.1.2 去除有毒物質 9
2.1.3 發泡劑 10
2.1.4 燃料 11
2.1.5 析出金屬 12
2.1.6 蝕刻液 12
2.2 不相容性反應 14
2.3 過氧化氫運輸與儲存準則 15
2.4 高等熱分析軟體 17
2.4.1 Friedman 等轉化率微分法 17
2.4.2 Flynn-Wall-Ozawa 反應動力學 19
2.4.3 Kissinger-Akahira-Sunose 昇溫熱反應動力學 21
第三章 實驗設備及研究方法 23
3.1 實驗流程 23
3.2 實驗設備及原理 24
3.2.1 微差掃描熱卡計 (Differential scanning calorimetry, DSC) 24
3.2.2 似絕熱試驗 27
3.2.3 多頻道微量熱卡計 (Thermal activity monitor III, TAM III) 28
3.2.4 高級熱分析軟體 32
3.3 實驗樣品 34
3.4 實驗條件 35
3.4.1 微差掃描熱卡計實驗流程 36
3.4.2 似絕熱試驗實驗流程 37
3.4.3 多頻道微量熱卡計實驗流程 38
第四章 結果與討論 39
4.1 DSC熱分析 39
4.2 似絕熱試驗 50
4.3 TAM III 分析 57
4.4 動力學分析 59
第五章 結論與建議 65
5.1 結論 65
5.2 建議 66
參考文獻 67




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