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研究生:何思穎
研究生(外文):Szu-Ying Ho
論文名稱:自酸蝕牙科黏著劑經老化測試之奈米級斷層掃描非破壞性分析與剪切黏著強度檢測
論文名稱(外文):Nondestructive Analysis on Dentin-adhesive-composite Interface by Nano-computed Tomography and Shear Bond Strength Evaluation of Self-etch Adhesives after Aging Tests
指導教授:姜昱至
指導教授(外文):Yu-Chih Chiang
口試委員:李伯訓林弘萍
口試委員(外文):Bor-Shiunn LeeHong-Ping Lin
口試日期:2021-06-21
學位類別:碩士
校院名稱:國立臺灣大學
系所名稱:臨床牙醫學研究所
學門:醫藥衛生學門
學類:牙醫學類
論文種類:學術論文
論文出版年:2021
畢業學年度:109
語文別:中文
論文頁數:66
中文關鍵詞:自酸蝕牙科黏著劑兩層塗抹兩倍時間塗抹冷熱循環老化測試奈米級電腦斷層掃描非破壞性分析剪切黏著強度
外文關鍵詞:self-etch adhesivedouble-coat applicationdouble-time applicationthermal cycling aging testnano CTNondestructive analysisshear bond strength
DOI:10.6342/NTU202103963
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目錄
中文摘要 i
ABSTRACT iii
目錄 vi
圖目錄 ix
表目錄 x
第一章 緒論 1
1.1 牙科黏著劑之發展 1
1.1.1 牙釉質黏著 1
1.1.2 牙本質黏著. 2
1.2 自酸蝕黏著劑之黏著強度影響因素文獻回顧 5
1.3 自酸蝕黏著劑不同操作方法之文獻回顧 7
1.3.1 兩次塗抹double-layer/ multilayer 7
1.3.2 兩層塗抹double-coat (2-coat). 9
1.3.3 兩倍時間塗抹double-time/double-application (2-time) 10
1.4 老化試驗 10
1.5 黏著介面之影像分析與觀察 11
第二章 實驗動機與目的 15
第三章 實驗材料與方法 16
3.1 自酸蝕黏著劑處理牙本質之酸鹼值與牙本質表面酸蝕分析 16
3.1.1 酸鹼值測試 16
3.1.2 牙本質表面酸蝕之觀察分析 19
3.2 黏著劑剪切黏著強度測試 21
3.2.1 測試樣品製備與分組 21
3.2.2 剪切黏著強度(SBS)測試 21
3.2.3 掃描式電子顯微鏡(SEM)觀察 22
3.3 牙本質-黏著劑-複合樹脂之黏著介面影像分析 23
3.3.1 掃描式電子顯微鏡(SEM)觀察 23
3.3.2 奈米級X光電腦斷層掃描(nano CT)分析 24
3.4 統計分析 27
第四章 實驗結果 28
4.1 黏著劑酸鹼值與牙本質表面酸蝕觀察分析 28
4.1.1 酸鹼值 28
4.1.2 牙本質表面酸蝕之觀察分析 28
4.1.2.1 掃描式電子顯微鏡(SEM) 28
4.1.2.2 能量散射X射線(EDS)分析 29
4.2 黏著劑剪切黏著強度測試與測試後斷裂介面影像 29
4.2.1 剪切黏著強度測試 29
4.2.2 掃描式電子顯微鏡(SEM)斷裂介面觀察 30
4.3 牙本質-黏著劑-複合樹脂之黏著介面影像分析 30
4.3.1 掃描式電子顯微鏡(SEM)黏著介面橫切面觀察 30
4.3.2 奈米級X光電腦斷層掃描(nano CT)分析 31
4.3.2.1 影像比較 31
4.3.2.2 VOI平均孔隙體積比率(volume fraction of porosity) 32
第五章 討論 33
5.1 不同廠牌黏著劑之差異探討 33
5.1.1 自酸蝕黏著劑pH值 33
5.1.2 自酸蝕黏著劑之成分 34
5.2 不同操作方式之影響探討 36
5.3 冷熱循環次數之影響 37
5.4 奈米級X光電腦斷層掃描(nano CT)分析 39
第六章 結論 44
第七章 未來研究方向 46
參考資料 47
圖目錄
圖4-1 51
圖4-2 51
圖4-3 52
圖4-4 52
圖4-5 53
圖4-6 53
圖4-7 54
圖4-8 55
圖4-9 56
圖4-10 57
圖4-11 58
圖4-12 59
圖4-13 60
圖4-14 61
圖4-15 62
圖4-16 63
表目錄
表4-1 不同處理方式之牙本質試片表面Ca/P ratio 64
表4-2 SBU與GPR於不同操作方式及冷熱循環次數之剪切黏著強度(SBS) 64
表4-3 理想鍵結強度比例QBS rate 65
表4-4 不同處理方式之牙本質試片表面Ca/P ratio 66
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