臺灣博碩士論文加值系統

摘要 i
Abstract iii
誌謝 vi
目錄 vii
表目錄 x
圖目錄 xi
第一章 緒論 1
1.1 前言 1
1.2 研究動機 5
第二章 文獻回顧 7
2.1 磷酸鋁黏著劑 7
2.2 磷鋁比 10
2.3 固化劑 15
2.3.1 金屬氧化物 15
2.3.2 固化劑的影響 16
2.4 剪切強度 22
2.5 耐溫性 25
2.5.1 高溫鍛燒 26
2.5.2 熱衝擊 28
2.5.3 熱循環 30
2.6 耐水性 32
第三章 實驗程序 35
3.1 實驗藥品 35
3.2 儀器設備 37
3.3 實驗步驟 42
3.3.1 磷酸二氫鋁之合成 42
3.3.2 磷酸鋁黏著劑之合成 43
3.3.3 磷鋁鋁黏著劑剪切試驗試片之製備及測試方法 46
第四章 結果與討論 50
4.1 磷酸鋁黏著劑的製備 50
4.1.1 不同磷鋁比之磷酸二氫鋁的合成 50
4.1.2 磷鋁比對磷酸鋁黏著劑力學性質的影響 52
4.2 固化劑的挑選 59
4.2.1 固化劑對磷酸鋁黏著劑熱性質的影響 59
4.2.2 固化劑對磷酸鋁黏著劑耐水性的影響 65
4.3 複合固化劑對磷酸鋁黏著劑的影響 72
4.3.1 複合固化劑之組成比例 72
4.3.2 複合固化劑對磷酸鋁黏著劑剪切強度的影響 74
4.4 磷酸鋁黏著劑的耐水性 78
4.5 磷酸鋁黏著劑之耐溫性 83
4.5.1 磷酸鋁黏著劑之耐高溫性及高溫下機械性質 83
4.5.2 磷酸鋁黏著劑之熱衝擊試驗 95
4.5.3 磷酸鋁黏著劑之熱循環試驗 97
第五章 結論 100
第六章 參考文獻 102

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