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研究生:游湘君
研究生(外文):Yu, Hsiang-Chun
論文名稱:利用鹽類研磨輔助共溶劑化學剝除法製備大橫向尺寸二硫化鉬奈米片
論文名稱(外文):Fabrication of Large-lateral Size MoS2 Nanosheets by Salt-assisted Mechanical Milling Process and Chemical Exfoliation in Cosolvent
指導教授:吳欣潔吳欣潔引用關係謝宗雍
指導教授(外文):Wu, Hsin-JayHsieh, Tsung-Eong
口試委員:江姿萱
學位類別:碩士
校院名稱:國立陽明交通大學
系所名稱:材料科學與工程學系所
學門:工程學門
學類:材料工程學類
論文種類:學術論文
論文出版年:2021
畢業學年度:110
語文別:英文
論文頁數:48
中文關鍵詞:二維材料大面積奈米片鹽類研磨輔助法化學剝除法二硫化鉬
外文關鍵詞:two-dimensional materialslarge-area nanosheetssalt-assisted milling processchemical exfoliationMoS2
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Abstract (in Chinese) ..................................................................................................... i
Abstract (in English) ......................................................................................................ii
Acknowledgments.........................................................................................................iv
Contents..........................................................................................................................v
Figure Captions ...........................................................................................................vii
Table Captions ...............................................................................................................x
Chapter 1 Introduction ..................................................................................................1
Chapter 2 Literature Review...........................................................................................4
2.1. CVD………………………………………………………………………….5
2.2. Hydrothermal Method………………………………………………………..6
2.3. Mechanical Exfoliation………………………………………………………8
2.4. Organolithium Exfoliation……………………………………………….......9
2.5. Liquid-Phase Exfoliation…………………………………………………...10
2.6. Salts and Surfactant/Polymer-Assisted Liquid-Phase Exfoliation…………12
2.7. Research Motivations………………………………………………………13
Chapter 3 Experimental Methods…………………………………………………….15
3.1. Experiment Flow…………………………………………………………....15
3.2. Preparation of Na2CO3-assisted MoS2 Powder and Dispersion…...…..……17
3.3. Characterizations…………………………………………………………....18
3.3.1. Structure Characterizations…………………….………………….....18
3.3.2. Optical, Zeta Potential Characterizations and Sedimentation
Experiment……………………….…………………………..………18
3.3.3. Thickness and Lateral Size Measurements…………………………..19
Chapter 4 Results and Discussion……………………………………………………20
4.1. The Influence of Salt-assisted Process…..……….………………………20
4.2. The Influence of Sonication Time……………...………………………....32
Chapter 5 Conclusions……………………………………………………………….38
Chapter 6 Perspective Works…………………………………………………...……40
References………………………………………………………………………..…..41
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