臺灣博碩士論文加值系統

致謝 i
摘要 ii
ABSTRACT iii
目錄 v
圖目錄 ix
表目錄 xii
1. 緒論 1
1.1 前言 1
1.2 動機與目的 2
1.3 研究架構 3
2. 理論基礎與文獻回顧 5
2.1 抗菌劑介紹 5
2.2 金屬和金屬氧化物的抗菌活性 6
2.2.1 Ag 和 Ag2O 奈米粒子 6
2.2.2 ZnO 奈米粒子 9
2.2.3 Cu 和 CuO 奈米粒子 10
2.3 層狀雙氫氧化物(LDHs)的介紹 12
2.3.1 基本結構與特性 13
2.3.2 製備方法 16
2.3.3 記憶效應 18
2.3.4 應用領域 19
2.4 菌種介紹 22
2.4.1 大腸桿菌 22
2.4.2 金色葡萄球菌 24
2.5 抑菌圈原理與介紹 26
3. 實驗方法與步驟 28
3.1 實驗藥品及設備 28
3.2 LDHs之製備 30
3.2.1 共沉澱法 30
3.2.2 水熱法 31
3.3 LDHs煅燒 32
3.4 圓盤擴散實驗 32
3.5 肉湯稀釋實驗 33
3.5.1 ANOVA 單向分析 34
3.5.2 Tukey-Kramer多重比較 35
3.6 材料特性鑑定 36
3.6.1 X光粉末繞射儀(XRD) 36
3.6.2 場發射掃描式電子顯微鏡(FESEM) 38
3.6.3 能量色散X-射線光譜(EDS) 39
3.6.3 雷射粒徑分析儀(DLS) 41
3.6.5 感應耦合電漿光學發射光譜儀(ICP-OES) 42
3.6.6 比表面積分析儀(BET) 43
4. 結果與討論 45
4.1 LDHs材料鑑定 45
4.1.1 XRD分析 45
4.1.2 SEM及EDS 分析 49
4.1.3 DLS 分析 53
4.1.4 ICP-OES分析 55
4.1.5 BET分析 56
4.2 圓盤擴散實驗分析 58
4.2.1 圓盤擴散法二元與三元材料之抑菌效應 58
4.2.2 圓盤擴散法銅的含量之抑菌效應 61
4.2.3 圓盤擴散法溫度煅燒之抑菌效應 63
4.2.4 肉湯稀釋實驗之抑菌效應 65
4.3 本研究系列LDHs抑菌劑抑菌效能評估 67
4.3.1 不同LDHs抑菌劑抑菌效能評估 68
4.4 LDHs抑菌機制 69
5. 結論與未來展望 71
5.1 結論 71
5.2 未來展望 73
參考文獻 74
自傳 86

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